Tetrahedron Letters p. 757 - 761 (2006)
Update date:2022-08-03
Topics:
Yoshizawa, Kazuhiro
Shioiri, Takayuki
1,3-Diaryl-2-propynyl trimethylsilyl ethers were easy to isomerize into the corresponding siloxyallenes using a catalytic amount of potassium tert-butoxide under very mild conditions. The siloxyallenes reacted in situ with various aldehydes to afford Z-selective β-branched Morita-Baylis-Hillman-type adducts in a one-pot reaction after acid treatment.
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