Tetrahedron Letters p. 403 - 406 (1999)
Update date:2022-08-03
Topics:
Thomas, James B.
Gigstad, Kenneth M.
Fix, Scott E.
Burgess, Jason P.
Cooper, Julie B.
Mascarella, S. Wayne
Cantrell, Buddy E.
Zimmerman, Dennis M.
Carroll, F. Ivy
A convergent, highly stereoselective synthetic approach to N-alkyl-4β- methyl-5-phenylmorphans has been developed utilizing alkylation of the metalloenamine of N-alkyl-1,2,3,6-tetrahydro-4-phenylpyridines with 2- (chloromethyl)-3,5-dioxahex-1-ene (Okahara's reagent) followed by Clemmensen reduction.
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