Journal of Organometallic Chemistry p. 283 - 290 (1984)
Update date:2022-08-02
Topics:
Arsenault, Clement
Bougeard, Peter
Sayer, Brian G.
Yeroushalmi, Shahin
McGlinchey, Michael J.
Treatment of the potassium salt of pentakis(carbomethoxy)cyclopentadiene with bromopentacarbonylmanganese(I) gives pentakis(carbomethoxy)cyclopentadienyltricarbonylmanganese(I) in good yield.Photochemical substitution of a metal carbonyl group by tributylphosphine, triphenylphosphine and triethyl phosphite is reported.Attempts to modify the ester function are described; hydrolysis or amination give mixed products but reduction with lithium aluminum hydride yields ultimately the pentamethylcyclopentadienyl complex.
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