Journal of Organic Chemistry p. 4866 - 4871 (1984)
Update date:2022-08-04
Topics:
White, Emil H.
Ribi, Max
Cho, Lee K.
Egger, Notker
Dzadzic, Petar M.
Todd, Michael J.
The nitrosation of N-alkyl-O-acylhydroxylamines leads to immediate decomposition at dry ice temperatures; the corresponding ester and nitrous oxide are formed.An 18O study has shown that the nitroso-O-acylhydroxylamines fragment directly rather than undergo a rearrangement reaction (as observed with the nitrosoamides).The product yields are respectable, especially at low tempreatures, and the method has promise for the generation of high energy carbonium ions.
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