REMOVAL OF SUGAR DITHIOACETAL GROUP WITH N-BROMOSUCCINIMIDE

DOI: 10.1016/0008-6215(84)85080-6

Source and publish data:

Carbohydrate Research p. 11 - 20 (1984)

Update date:2022-08-04

Topics: Experimental terms Article N-bromosuccinimide Removal

Authors:

Miljkovic, Momcilo

Dropkin, Daniel

Hagel, Peter

Habash-Marino, Margaret

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Article abstract of DOI:10.1016/0008-6215(84)85080-6

Oxidative removal of the dithioacetal group of several protected sugar and 2-acylamido-2-deoxy sugar dialkyl dithioacetals with N-bromosuccinimide in 97percent aqueous acetone or 1:1 (v/v) 2-methyl-2-propanol-acetone was compared with removal with mercury dichloride-mercury(II) oxide or mercury dichloride-cadmium carbonate.In general, removal with N-bromosuccinimide proceeded more rapidly, and, with one exception, yields higher than or equal to those obtained with the method using mercury salt.

Full text of DOI:10.1016/0008-6215(84)85080-6

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