Carbohydrate Research p. 11 - 20 (1984)
Update date:2022-08-04
Topics: Experimental terms Article N-bromosuccinimide Removal
Miljkovic, Momcilo
Dropkin, Daniel
Hagel, Peter
Habash-Marino, Margaret
Oxidative removal of the dithioacetal group of several protected sugar and 2-acylamido-2-deoxy sugar dialkyl dithioacetals with N-bromosuccinimide in 97percent aqueous acetone or 1:1 (v/v) 2-methyl-2-propanol-acetone was compared with removal with mercury dichloride-mercury(II) oxide or mercury dichloride-cadmium carbonate.In general, removal with N-bromosuccinimide proceeded more rapidly, and, with one exception, yields higher than or equal to those obtained with the method using mercury salt.
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