Journal of the Chemical Society. Chemical communications p. 1137 - 1138 (1985)
Update date:2022-07-29
Topics:
Yoshida, Toshikatsu
Ueda, Tatsuo
Adachi, Tomohiro
Yamamoto, Kazuhiko
Higuchi, Taiichi
Two conformers for the cationic rhodium(I) complexes of the title 14-membered cyclic tetrasulphides have been prepared on the conformational effect upon the nucleophilicity of rhodium(I) ion is shown by the oxidative addition reaction of CH2Cl2; (Rh<14>aneS4)Cl (1), in which the Rh atom lies 0.133(2) Angstroem above the plane of four S atoms, forms a dimer through a Rh...Rh <3.313(1) Angstroem> and four Rh...S <3.697(9)-3.822(3) Angstroem> intermolecular non-bonded interactions as established by an X-ray crystal structure determination.
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