Journal of Organic Chemistry p. 7739 - 7746 (1995)
Update date:2022-08-24
Topics:
Moss, Robert A.
Bracken, Kathryn
Emge, T. J.
9-Iodoso-10-phenanthroic acid (IPA-OH) was prepared from 9-cyanophenanthrene in a four-step, 44percent overall yield synthesis, featuring cyano-directed ortho lithiation/iodination as the key step.An X-ray crystal structure showed that IPA-OH exsists in a
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