Bulletin of the Chemical Society of Japan p. 1035 - 1038 (1988)
Update date:2022-08-16
Topics:
Kitajima, Nobumasa
Takemura, Kazuya
Moro-Oka, Yoshihiko
Yoshikuni, Tadatsugu
Akada, Mitsuo
et al.
The selective liquid-phase oxidation of 3,4,5-trimethoxytoluene to 3,4,5-trimethoxybenzaldehyde, an important chemical intermediate for medicine production, was developed; when 2.0 mmol of the reactant was heated at 110 deg C for 2 h in an autoclave under 3 atm O2 with 10 ml of acetic acid in the presence of 0.75 mmol of Co(OAc)2-Mn(OAc)2 (3:1 mol ratio), a 92percent yield of the aldehyde was obtained.
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