Organometallics p. 1674 - 1676 (1988)
Update date:2022-08-10
Topics:
Strickland, Debra S.
Wilson, Scott R.
Shapley, John R.
Photolyzing a mixture of Re2(CO)10 and H3Os3(CO)9(μ3-CBr) under CO (～2 atm) is a convenient method of generating the radical H3Os3(CO)9(μ3-C ?). This species abstracts hydrogen from cyclohexane and toluene and adds to benzene. In deuteriated hydrocarbons H3Os3(CO)9(μ3-CD) is produced, but in cyclohexane-d12 a diketone complex, [H3Os3(CO)9(μ3-CCO)]2, also is formed.
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(1994)
