Journal of labelled compounds and radiopharmaceuticals p. 493 - 496 (1995)
Update date:2022-08-17
Topics:
Waehaelae, Kristiina
Vaeaenaenen, Tiina
Hase, Tapio
Leinonen, Antti
Isotopically pure d5-epitestosterone has been synthesized for the first time.This polydeuterated 17α-hydroxyandrosterone was prepared by H/D exchange reaction with MeOD-D2O under basic conditions.Its characteristics are described in detail, including its enolization into a d4-heterodienic silyl ether derivative upon silylation.Keywords: <2H>5-17α-Hydroxyandrost-4-en-3-one, d5-epitestosterone, deuteration, labeling, synthesis, dienolsilyl ether
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