Journal of the Chemical Society. Perkin Transactions 2 (2001) p. 2611 - 2613 (1996)
Update date:2022-08-31
Topics:
Perlikowska, Wieslawa
Modro, Agnes M.
Modro, Tomasz A.
Mphahlele, Malose J.
The lithiation of diethyl trichloromethylphosphonate below -100 °C leads to a stable α-lithiated derivative, but at temperatures of about -80 °C the lithiation is accompanied by spontaneous reactions leading to tetraethyl (chloromethylene)bisphosphonate as the exclusive product. Possible mechanisms of the reaction are discussed.
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