Journal of Organometallic Chemistry p. 9 - 14 (1980)
Update date:2022-08-11
Topics:
Sonnek, Georg
Mueller, Gisela
Baumgarten, Karl-Guenther
Treatment of sulphur trioxide with tris(silylalkyl)aluminium compounds followed by hydrolysis and extraction with ethyl alcohol is a new method for preparation of substituted sodium silylalkane sulphonates.Weak donor-acceptor complexes of the starting compounds react selectively with insertion at the aluminium-carbon bond without cleavage of the silicon-carbon bond.The structure of the silylalkane sulphonates is determined by 1H NMR and IR spectroscopy.
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