Tetrahedron Letters p. 3487 - 3490 (1993)
Update date:2022-08-17
Topics:
Guijarro, Albert
Yus, Miguel
The reaction of an equimolar amount of chloromethyl ethyl ether (1) and different carbonyl compounds (2) with an excess of lithium powder (1:7 molar ratio) in the presence of a catalytic amount of 4,4′-di-tert-butylbiphenyl (5 mol %) in THF at 0°C leads, after hydrolysis, to the corresponding hydroxyethers 3.
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