Tetrahedron Letters p. 7845 - 7848 (1995)
Update date:2022-08-18
Topics:
Bennua-Skalmowski
Krolikiewicz
Vorbrueggen
Persilylation of excess D-ribose or D-glucose with 6-azauracil or N6-benzoyl-adenine followed by condensation with trimethylsilyl triflate in acetonitrile at 80° affords the corresponding persilylated nucleosides. Transsilylation with methanol and chromatography on SiO2 give the pure free nucleosides in up to 70% yield.
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