Tetrahedron Letters p. 2141 - 2144 (1999)
Update date:2022-08-11
Topics:
Doi, Takayuki
Sugiki, Masayuki
Yamada, Haruo
Takahashi, Takashi
Porco Jr., John A.
Glycosidation of silicon-connected glycosyl donors on polystyrene resin is described Thiophenyl glycoside 2a and glucopyranosyl fluoride 2b reacted with glycosyl acceptor 3 (R2 = Bn) to give disaccharide 4a in 96% and 70% yields, respectively. Glycosidation of thiophenyl glucoside 2a (R1 = Bn or Bz) with glycosyl acceptor 3 (R2 = Bn or Ac) yielded 4a-4c in satisfactory yields and 4d in moderate yield.
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