Monatshefte fur Chemie p. 565 - 568 (1995)
Update date:2022-08-16
Topics:
Tran-Thi, N. H.
Falk, H.
A high yield synthesis of 1-triacontanol was based on the cheap and easily available starting materials 1-octadecanol and 1,12-dodecanediol.The first one was converted to octadecanal using a phase transfer system, whereas the second one after phase transfer bromination and reaction with triphenylphosphine provided 1-hydroxy-12-triphenylphosphonium bromide.Wittig reaction of these two synthons and subsequent hydrogenation furnished the desired product. - Keywords: 1-Triacontanol: Wittig reaction; Phase transfer reaction; Plant growth hormone
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