1,2-dimethoxycyclohexane

Base Information

• Chemical Name: 1,2-dimethoxycyclohexane
• CAS No.: 19752-95-5
• Molecular Formula: C₈H₁₆O₂
• Molecular Weight: 144.214
• Mol file: 19752-95-5.mol

Synonyms:1,2-dimethoxycyclohexane

Chemical Property of 1,2-dimethoxycyclohexane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1,2-dimethoxycyclohexane

There total 17 articles about 1,2-dimethoxycyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

methanol (67-56-1) + trans-1-methoxy-2-phenylselenocyclohexane (51533-22-3) → 1,2-dimethoxycyclohexane (19752-95-5)

Guidance literature:

With naphthalene-1,4-dicarbonitrile; Irradiation;

DOI:10.1021/ja00170a045

Reference yield: 47.0%

1,2-dimethoxybenzene (91-16-7) → 2-methoxycyclohexane (931-56-6) + cyclohexane (110-82-7,25012-93-5) + 1,2-dimethoxycyclohexane (19752-95-5) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + cyclohexanol (108-93-0)

Guidance literature:

With 5% active carbon-supported ruthenium; hydrogen; magnesium oxide; In water; at 159.84 ℃; for 2h; under 11251.1 Torr;

DOI:10.1039/c3gc42322k

Reference yield: 42.0%

methanol (67-56-1) + cyclohexene (110-83-8) → cyclopentanealdehyde (872-53-7) + 3-methoxycyclohexene (2699-13-0) + 1,2-dimethoxycyclohexane (19752-95-5)

Guidance literature:

With [bis(acetoxy)iodo]benzene; sulfuric acid; at -15 ℃; for 2.33333h;

DOI:10.1007/s11172-005-0027-8

upstream raw materials:

1,2-Cyclohexanediol

methyl iodide

methanol

trans-1-methoxy-2-phenylselenocyclohexane

Downstream raw materials:

(3,4-dimethoxyphenyl)phenylmethane