CAS No.100-60-7,N-Methylcyclohexylamine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	100-60-7
Name:	N-Methylcyclohexylamine
Article Data:	99

Formula:	C₇H₁₅N
Molecular Weight:	113.203
Synonyms:	Cyclohexylamine,N-methyl- (6CI,7CI,8CI);(Methylamino)cyclohexane;Cyclohexylmethylamine;Methylcyclohexylamine;N-Cyclohexyl-N-methylamine;N-Cyclohexylmethylamine;N-Methyl-N-cyclohexylamine;N-Methylcyclohexanamine;NSC 434;
EINECS:	202-869-3
Density:	0.868 g/cm³
Melting Point:	-9--7 °C(lit.)
Boiling Point:	146.5 °C at 760 mmHg
Flash Point:	29.4 °C
Solubility:	5.4 g/100 mL (20 °C) in water
Appearance:	clear colourless to yellow liquid
Hazard Symbols:	C
Risk Codes:	10-21/22-35-20/21/22
Safety:	16-26-36/37/39-45
Transport Information:	UN 2734 8/PG 2
PSA:	12.03000
LogP:	1.92940

Synthetic route

: 108-94-1
cyclohexanone

: 124-40-3
dimethyl amine

A: 100-60-7
N-methylcyclohexylamine

B: 98-94-2
N,N-dimethyl-cyclohexanamine

C: 108-93-0
cyclohexanol

Conditions

Conditions	Yield
With hydrogen at 160 - 220℃; under 67506.8 - 97509.8 Torr; for 100 - 1000h; Product distribution / selectivity;	A 0.1% B 96% C 0.5%
With hydrogen at 160 - 180℃; under 63756.4 - 97509.8 Torr; for 100 - 400h; Product distribution / selectivity;	A 0.1% B 94% C 2%

...Expand

: 109-73-9
N-butylamine

: 3-methyl-2-(N-methylcyclohexylamino)benzothiazolium iodide

A: 70038-63-0
butyl-(3-methyl-3H-benzothiazol-2-ylidene)-amine

B: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
at 25℃; for 3h;	A 95% B 83%
In dichloromethane at 25℃; for 3h;	A 95% B 83%

...Expand

: 931-53-3
Cyclohexyl isocyanide

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With Zr12(μ3-O)5[(μ3-O)CoCl]8[(μ2-O)2(μ3-O)CoCl]3Li3(triphenyldicarboxylate)9; hydrogen In toluene at 110℃; under 30003 Torr; for 42h; Catalytic behavior; Inert atmosphere; Schlenk technique;	92%
With dimethyl sulfoxide In water at 100℃; Green chemistry;	65%

: 100-61-8
N-methylaniline

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With hydrogen In neat (no solvent) at 80℃; under 7600.51 Torr; for 24h; Catalytic behavior; Autoclave;	91%
With dichloro(μ-chloro)(μ-hydrido)bis(η-p-cymene)diruthenium(II); hydrogen In neat (no solvent) at 75℃; under 37503.8 Torr; for 24h;	80%
With lithium; methylamine

: 593-51-1
methylamine hydrochloride

: 108-94-1
cyclohexanone

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With iridium bromide; zinc In 1,4-dioxane; water at 30℃; for 72h;	85%
With titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 10 h, 2.) EtOH, 25 deg C, 8 h; Yield given. Multistep reaction;

: 108-94-1
cyclohexanone

: 74-89-5
methylamine

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With hydrogenchloride; Zr(BH4)2Cl2(dabco)2 In methanol for 1h; Heating;	78%
With D-glucose; glucose dehydrogenase CDX-901; imine reductase 48 from Rhizobium sullae; nicotinamide adenine dinucleotide phosphate In aq. buffer at 25℃; for 24h; pH=9; Enzymatic reaction;	66%
With sodium tetrahydroborate; lithium chloride In tetrahydrofuran; methanol Flow reactor; chemoselective reaction;	37%

: 67-56-1
methanol

: 108-91-8
cyclohexylamine

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With rhodium(III) chloride hydrate; potassium tert-butylate at 130℃; for 48h; Sealed tube; High pressure;	75%
With thorium dioxide at 320℃;
rhodium hydrido (PEt3)3 complex for 10h;	99 % Chromat.
With platinum on carbon; hydrogen; sodium hydroxide at 130℃; under 30003 Torr; for 36h; Autoclave;	74 %Chromat.
With palladium 10% on activated carbon; potassium tert-butylate at 130℃; for 12h;

: 141339-38-0
N-(6-Methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-N-methyl-hydroxylamine

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With carbon disulfide In acetonitrile for 1.5h; Ambient temperature;	71%

: 15267-95-5
chloromethyltriethoxysilane

: 108-91-8
cyclohexylamine

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
Stage #1: chloromethyltriethoxysilane; cyclohexylamine at 87℃; for 18h; Stage #2: With water In ethanol for 48h; Heating; Further stages.;	68%

: Cyclohexyl-phenylsulfanylmethyl-amine; hydrochloride

: 100-60-7
N-methylcyclohexylamine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In diethyl ether -60 degC -> room temp.;	67%

Raw Materials

108-94-1

121-69-7

98-95-3

6257-10-9

2739-12-0

519-73-3

100-61-8

124-68-5

Downstream Products

519-73-3

108-94-1

98-94-2

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Chemistry

MF: C₇H₁₅N
MW: 113.2
EINECS: 202-869-3
mp -9 ~ -7 °C(lit.)
bp 149 °C(lit.)
density 0.868 g/mL at 25 °C(lit.)
vapor density 4 (vs air)
vapor pressure 11 mm Hg ( 40 °C)
refractive index n20/D 1.456(lit.)
Fp 85 °F
storage temp. Flammables area
Water Solubility 5.4 g/100 mL (20 ^oC)
Sensitive Air Sensitive

Toxicity Data With Reference

RTECS GX1529000

Safety Profile

Hazard Codes C
Risk Statements 10-21/22-35-20/21/22
Safety Statements 16-26-36/37/39-45
RIDADR UN 2734 8/PG 2
WGK Germany 1
Hazard Note Corrosive
HazardClass 8