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139-02-6

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Basic Information
CAS No.: 139-02-6
Name: Phenol, sodium salt(1:1)
Molecular Structure:
Molecular Structure of 139-02-6 (Phenol, sodium salt(1:1))
Formula: C6H6 O . Na
Molecular Weight: 116.10
Synonyms: Phenol,sodium salt (8CI,9CI); Sodium phenoxide (6CI); Phenol sodium; Sodium carbolate;Sodium phenate; Sodium phenolate; Sodium phenylate
EINECS: 205-347-3
Density: 0,898 g/cm3
Melting Point: >300℃
Boiling Point: 181.8 °C at 760 mmHg
Flash Point: 28°C
Solubility: Very soluble in water, soluble in alcoholSoluble in water, acetone and alcohol.
Appearance: white like or light brown crystalline powder
Hazard Symbols: Strong irritant to skin and tissue.
Risk Codes: 34
Safety: Poison by subcutaneous route. A corrosive irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of Na2O. See also PHENOL and SODIUM HYDROXIDE.
Transport Information:
PSA: 23.06000
LogP: 1.83040
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102-09-0

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139-02-6

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Conditions
ConditionsYield
With water; sodium hydroxide In dimethyl sulfoxide at 25℃; Kinetics;A 100%
B n/a
108-95-2

phenol

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide In methanol; water98.9%
With sodium In 1,4-dioxane for 4h; Heating;92%
With methanol; sodium
1121-70-6

sodium 4-methylphenoxide

poly(styrene p-tolyliodonium) hydrogensulfate

poly(styrene p-tolyliodonium) hydrogensulfate

139-02-6

sodium phenoxide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃; for 24h;65%
122-99-6

2-Phenoxyethanol

A

139-02-6

sodium phenoxide

B

3598-16-1

2-phenoxyacetic acid sodium salt

Conditions
ConditionsYield
With oxygen; bismuth(III) nitrate; palladium on activated charcoal In sodium hydroxide at 90℃; for 6h; Product distribution; also with coactivator and other activators, various times, reaction with other 2-phenoxyethanols;A n/a
B 53%
67-56-1

methanol

10113-28-7

dimethyl phenyl phosphate

124-41-4

sodium methylate

A

512-56-1

trimethyl phosphite

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 0℃; Rate constant;
at 19℃; Rate constant;
at 10℃; Rate constant;
...Expand
60-29-7

diethyl ether

64-17-5

ethanol

13400-05-0

trichloro-methanesulfenic acid phenyl ester

141-52-6

sodium ethanolate

A

13029-05-5

trichloro-methanesulfenic acid ethyl ester

B

139-02-6

sodium phenoxide

...Expand
64-17-5

ethanol

1247-19-4

diphenyldiphenoxysilane

furan-2,3,5(4H)-trione pyridine (1:1)

A

512-63-0

1,1,3,3,5,5-hexaphenylcyclotrisiloxane

B

139-02-6

sodium phenoxide

...Expand
339199-98-3

1,3,5-trinitro-2,4,6-triphenoxy-benzene

141-52-6

sodium ethanolate

A

68959-41-1

1,3,5-triethoxy-2,4,6-trinitrobenzene

B

139-02-6

sodium phenoxide

...Expand
110-54-3

hexane

676-54-0

ethyl sodium

100-66-3

methoxybenzene

139-02-6

sodium phenoxide

...Expand
1247-19-4

diphenyldiphenoxysilane

furan-2,3,5(4H)-trione pyridine (1:1)

67-64-1

acetone

A

512-63-0

1,1,3,3,5,5-hexaphenylcyclotrisiloxane

B

139-02-6

sodium phenoxide

...Expand
110-54-3

hexane

676-54-0

ethyl sodium

103-73-1

Phenetole

139-02-6

sodium phenoxide

...Expand
623-11-0

1-methyl-4-nitrosobenzene

98-11-3

benzenesulfonic acid

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 310 - 360℃; Rate constant;
70310-90-6

N,N'-bis(diphenyloxyphosphonyl)-8-quinolinesulfinamidine

A

139-02-6

sodium phenoxide

B

64326-13-2

sodium naphthalene-1-sulfinate

Conditions
ConditionsYield
With sodium hydroxide for 3h; Product distribution; Heating;
93-99-2

benzoic acid phenyl ester

A

532-32-1

sodium benzoate

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane; water at 15℃; Rate constant; Thermodynamic data; Kinetics; var. temperatures, var. ratio of solvents, log A, Ea;
2122-46-5, 55748-05-5

phenoxy radical

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With Sodium borate; sodium azide; oxygen; sodium formate In water Rate constant; Irradiation; combination with superoxid anion radicals;
20376-70-9

phenyl N-methyl-N-m-nitrophenylcarbamate

A

619-26-1

N-methyl-3-nitroaniline

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide; cetyltrimethylammonim bromide In methanol; water at 68.5℃; Rate constant; Mechanism; other N-methyl-N-arylcarbamates; reaction in absence of cetyltrimethylammonium bromide;
50882-34-3

Methyl-(4-nitro-phenyl)-carbamic acid phenyl ester

A

139-02-6

sodium phenoxide

B

100-15-2

N-methyl(p-nitroaniline)

Conditions
ConditionsYield
With sodium hydroxide; cetyltrimethylammonim bromide In methanol; water at 68.5℃; Rate constant;
3229-70-7

phenolate

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium cation In water; dimethyl sulfoxide at 25℃; Equilibrium constant;
3046-27-3

sodium m-chlorophenoxide

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium tetrahydroborate; hydrogen; PdCl2 complex on modified silca gel In methanol at 20℃; under 760 Torr; Rate constant; hydrogenolysis of chlorobenzenes in the presence of palladium chloride complex deposited on modified silica gel; effect of the nature of substituents in aromatic ring;
30616-32-1

1-phenylcarbamoyl-1-methylhydrazine

A

139-02-6

sodium phenoxide

B

C2H5N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; enegy parameters calculated from kobs in range 25-60 deg C; pH range 12.7, 13.9;
18197-54-1

N',N'-Dimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C3H7N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 12.0, 14.9;

N,N'-Dimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C3H7N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 13.0, 13.9;

N,N',N'-Trimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C4H9N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 13.6, 14.1;
20605-43-0

phenyl hydrazinecarboxylate

A

139-02-6

sodium phenoxide

B

CH3N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Thermodynamic data; Mechanism; energy parameters calculated from kobs in range 25-60 deg C; pH range 11.9, 14.9;
100-66-3

methoxybenzene

aqueous NaOH

aqueous NaOH

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 250 - 260℃;
110-86-1

pyridine

100-66-3

methoxybenzene

sodium

sodium

139-02-6

sodium phenoxide

...Expand
60-29-7

diethyl ether

7664-41-7

ammonia

100-66-3

methoxybenzene

sodium

sodium

139-02-6

sodium phenoxide

...Expand
60-29-7

diethyl ether

sodium amide

122-79-2

Phenyl acetate

A

60-35-5

acetamide

B

139-02-6

sodium phenoxide

...Expand

sodium amide

122-79-2

Phenyl acetate

71-43-2

benzene

A

60-35-5

acetamide

B

139-02-6

sodium phenoxide

...Expand
142-82-5

n-heptane

1822-71-5

n-pentylsodium

103-73-1

Phenetole

A

139-02-6

sodium phenoxide

B

2-ethoxy-phenyl sodium

2-ethoxy-phenyl sodium

Conditions
ConditionsYield
at 35℃; Product distribution;
at 75℃; Product distribution;
...Expand
111-83-1

1-bromo-octane

139-02-6

sodium phenoxide

1818-07-1

octyloxybenzene

Conditions
ConditionsYield
poly<1-hydroxyethylene-co-1-(2-ethylsulf In 1,4-dioxane at 75℃; for 23h; Product distribution; Rate constant; other catalysts;100%
Sucrose-ethyleneoxide adducts In toluene at 110℃; for 8h; Product distribution; further catalysts: PEG, DB18K6; further objects of study: phase-transfer catalysis;100%
dodecyldimethylsulfonium methyl sulfate In water at 40℃; for 6h;25%
623-00-7

4-bromobenzenecarbonitrile

139-02-6

sodium phenoxide

3096-81-9

4-phenoxybenzonitrile

Conditions
ConditionsYield
With potassium phosphate In tetrahydrofuran at 115℃; for 18h;100%
With CF3-DPPF; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 20h;79.6%
With CF3-DPPF ligand; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 30h; Product distribution; various DPPF ligands for the Pd-catalyzed formation of diaryl ethers;
139-02-6

sodium phenoxide

13790-39-1

6,7-dimethoxy-4-chloroquinazoline

1180653-47-7

6,7-dimethoxy-4-phenoxyquinazoline

Conditions
ConditionsYield
In dimethyl sulfoxide at 80℃; for 3h;100%
3360-41-6

4-phenyl-butan-1-ol

139-02-6

sodium phenoxide

358349-92-5

(4-phenoxybutyl)benzene

Conditions
ConditionsYield
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere;
Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere;		100%
31643-49-9

4-Nitrophthalonitrile

139-02-6

sodium phenoxide

38791-62-7

4-phenoxyphthalonitrile

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 1h;99%
1623-05-8

perfluoro(propyl vinyl ether)

139-02-6

sodium phenoxide

144373-62-6

(2-Chloro-1,1,2-trifluoro-2-heptafluoropropyloxy-ethoxy)-benzene

Conditions
ConditionsYield
With hexachloroethane In N,N-dimethyl-formamide 1) 25 deg C - 29 deg C, 2) r.t., overnight;99%
41663-84-7

4-nitro-N-methyl-phthalimide

139-02-6

sodium phenoxide

63197-24-0

4-phenoxy-N-methyl phthalimide

Conditions
ConditionsYield
N-neopentyl chloride of 4-dibutylaminopyridine In toluene at 110℃; for 1h;99%
In dimethyl sulfoxide at 15 - 120℃; for 24h; Inert atmosphere;93%

dimethyl-3-sulfopropyl(ferrocenylmethyl)ammonium

139-02-6

sodium phenoxide

hydroxymethylferrocene ethyl ether

Conditions
ConditionsYield
In water a mixt. of Fe compd. and C6H5ONa in water is refluxed for 5 min; mixt. is cooled and extd. with ether, extract is washed with ether and dried with sodium sulfate, removal of ether by distillation, recrystn. from heptane;99%
139-02-6

sodium phenoxide

83-01-2

diphenylcarbamic chloride

5416-45-5

diphenyl-carbamic acid phenyl ester

Conditions
ConditionsYield
at 20℃; for 0.08h; Neat (no solvent); Microwave irradiation; Grinding;99%
1610679-61-2

tert-butyl (3-bromo-5-chloropyrazolo[1,5-a]pyrimidin-7-yl)(2-morpholinoethyl)carbamate

139-02-6

sodium phenoxide

1610680-02-8

tert-butyl (3-bromo-5-phenoxypyrazolo[1,5-a]pyrimidin-7-yl)(2-morpholinoethyl)carbamate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 0.5h;99%
79696-96-1

2-Amino-6-chlor-3,4,5-pyridintricarbonitril

139-02-6

sodium phenoxide

2-Amino-6-phenoxy-3,4,5-tricyanopyridin

Conditions
ConditionsYield
In acetone for 0.5h; Heating;98%
139-02-6

sodium phenoxide

4-chloro-3-methylbut-2-enal dimethylacetal

1,1-dimethoxy-3-methyl-4-phenoxybut-2-ene

Conditions
ConditionsYield
In tetrahydrofuran; water for 48h; Ambient temperature;98%
139-02-6

sodium phenoxide

318956-66-0

C30H29Cl4N5O2P4S3

C54H49N5O6P4S3

Conditions
ConditionsYield
In tetrahydrofuran at 20℃;98%

C46H55NO5S

139-02-6

sodium phenoxide

C45H53NO3

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃;98%
139-02-6

sodium phenoxide

19579-04-5

tetrachlorophenoxyphosphorane

Conditions
ConditionsYield
With phosphorus pentachloride In tetrachloromethane at -15℃; for 1h;98%
3597-91-9

biphenyl-4-yl methanol

139-02-6

sodium phenoxide

29263-69-2

1-phenyl-4-phenoxymethylbenzene

Conditions
ConditionsYield
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere;
Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere;		98%
100-67-4

potassium phenolate

139-02-6

sodium phenoxide

1184-10-7

2,2,4,4,6,6-hexaphenoxycyclotriphosphazene

Conditions
ConditionsYield
With cesium hydroxide; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine In 1,2-dichloro-benzene at 175℃; Product distribution / selectivity;97.9%
139-02-6

sodium phenoxide

79-11-8

chloroacetic acid

108-95-2

phenol

122-59-8

2-phenoxyacetic acid

Conditions
ConditionsYield
at 105℃; pH=9 - 10;97.6%
...Expand
139-02-6

sodium phenoxide

96-34-4

methyl chloroacetate

2065-23-8

methyl 2-phenoxyacetate

Conditions
ConditionsYield
at 120℃; for 6h; Temperature;97.5%
17455-13-9

18-crown-6 ether

139-02-6

sodium phenoxide

C12H24O6*3C6H5O(1-)*3Na(1+)

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 1h; Ambient temperature;97%
139-02-6

sodium phenoxide

350-46-9

4-Fluoronitrobenzene

620-88-2

4-nitrophenyl phenyl ether

Conditions
ConditionsYield
N-2-ethylhexyl chloride of 4(4-methylpiperidinyl)pyridine In toluene at 110℃; for 0.25h;97%
With ammonia at 25℃; Kinetics; Concentration;

(7-methoxy[2.2]paracyclophan-4-yl)(4'-methoxyphenyl)iodonium hexafluorophosphate

139-02-6

sodium phenoxide

A

1655-69-2

1-methoxy-4-phenoxy-benzene

B

1235887-94-1

4-methoxy-7-iodo[2.2]paracyclophane

Conditions
ConditionsYield
In [D3]acetonitrile at 80℃; for 1h; Inert atmosphere; Darkness; regioselective reaction;A 75%
B 97%
...Expand
1313436-04-2

(S)-(1-benzyl-2,5-dihydro-1H-pyrrol-2-yl)methanol

139-02-6

sodium phenoxide

1313435-87-8

(R)-1-benzyl-3-phenoxy-1,2,3,6-tetrahydropyridine

Conditions
ConditionsYield
Stage #1: (S)-(1-benzyl-2,5-dihydro-1H-pyrrol-2-yl)methanol With trifluoromethylsulfonic anhydride In dichloromethane at -15℃; Inert atmosphere;
Stage #2: sodium phenoxide In tetrahydrofuran; dichloromethane at -15 - 20℃; Inert atmosphere; optical yield given as %ee; regioselective reaction;		97%

C29H36ClIrP2S2

139-02-6

sodium phenoxide

C35H41IrOP2S2

Conditions
ConditionsYield
In dichloromethane at 20℃; for 36h; Inert atmosphere; Glovebox;97%

4-(bromomethyl)-1,3-bis(2,6-diisopropylphenyl)-1,2,3-triazolium hexafluorophosphate

139-02-6

sodium phenoxide

1,3-bis(2,6-diisopropylphenyl)-4-(phenoxymethyl)-1,2,3-triazolium hexafluorophosphate

Conditions
ConditionsYield
In water; acetone at 20℃; for 12h; Schlenk technique;97%
1698-53-9

4,5-dichloro-1-phenylpyridazin-6-one

139-02-6

sodium phenoxide

38387-54-1

5-chloro-4-phenoxy-2-phenyl-2H-pyridazin-3-one

Conditions
ConditionsYield
In 1,4-dioxane for 16h; Ambient temperature;96%
64891-77-6

(2-13C)bromoacetic acid

139-02-6

sodium phenoxide

134757-64-5

<2-13C>-2-phenoxyacetic acid

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 2h; Heating;96%
60410-77-7

bis(4-methylbenzenethiocarbonyl) sulphide

139-02-6

sodium phenoxide

52322-79-9

O-phenyl 4-methylbenzenecarbothioate

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether; ethanol for 3h; Ambient temperature;96%
Raw Materials
67-56-1
1822-71-5
3229-70-7
1463-10-1
122-99-6
588-63-6
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7664-41-7
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19928-57-5
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458-92-4
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    China (Mainland)  |  Contact Details

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    Business Type:Manufacturers

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    139-02-6

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Chemistry

Synonyms: PHENOL,sodiumsalt;PHENOL,sodiumsalt(solid);PHENOLatesodium;PHENOLsodium;PHENOLsodiumsalt;sodiumcarbolate;sodiumPHENOLate,solid;SODIUM PHENATE
SODIUM PHENOXIDE is the chemical compound with the formula C6H5NaO.Its molar mass is 116.09.
density:0,898 g/cm3
Flash point:28°C
storage temp.:below 5° C
Sensitive:Hygroscopic

Toxicity Data With Reference

1.   

scu-mus LDLo:350 mg/kg

   AEXPBL    Archiv fuer Experimentelle Pathologie und Pharmakologie. 52 (1905),220.
2.   

scu-frg LDLo:100 mg/kg

   AEXPBL    Archiv fuer Experimentelle Pathologie und Pharmakologie. 52 (1905),220.

Consensus Reports

Sodium PHENOXIDE's reported in EPA TSCA Inventory.

Safety Profile

Poison by subcutaneous route. A corrosive irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of Na2O. See also PHENOL and SODIUM HYDROXIDE.

Standards and Recommendations

DOT Classification:  8; Label: Corrosive