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139-02-6

Basic Information
CAS No.: 139-02-6
Name: Phenol, sodium salt(1:1)
Molecular Structure:
Molecular Structure of 139-02-6 (Phenol, sodium salt(1:1))
Formula: C6H6 O . Na
Molecular Weight: 116.10
Synonyms: Phenol,sodium salt (8CI,9CI); Sodium phenoxide (6CI); Phenol sodium; Sodium carbolate;Sodium phenate; Sodium phenolate; Sodium phenylate
EINECS: 205-347-3
Density: 0,898 g/cm3
Melting Point: >300℃
Boiling Point: 181.8 °C at 760 mmHg
Flash Point: 28°C
Solubility: Very soluble in water, soluble in alcoholSoluble in water, acetone and alcohol.
Appearance: white like or light brown crystalline powder
Hazard Symbols: Strong irritant to skin and tissue.
Risk Codes: 34
Safety: Poison by subcutaneous route. A corrosive irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of Na2O. See also PHENOL and SODIUM HYDROXIDE.
Transport Information:
PSA: 23.06000
LogP: 1.83040
Synthetic route
102-09-0

bis(phenyl) carbonate

A

139-02-6

sodium phenoxide

B

81256-74-8

sodium salicylat

Conditions
ConditionsYield
With water; sodium hydroxide In dimethyl sulfoxide at 25℃; Kinetics;A 100%
B n/a
108-95-2

phenol

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide In methanol; water98.9%
With sodium In 1,4-dioxane for 4h; Heating;92%
With methanol; sodium
1121-70-6

sodium 4-methylphenoxide

poly(styrene p-tolyliodonium) hydrogensulfate

poly(styrene p-tolyliodonium) hydrogensulfate

139-02-6

sodium phenoxide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃; for 24h;65%
122-99-6

2-Phenoxyethanol

A

139-02-6

sodium phenoxide

B

3598-16-1

2-phenoxyacetic acid sodium salt

Conditions
ConditionsYield
With oxygen; bismuth(III) nitrate; palladium on activated charcoal In sodium hydroxide at 90℃; for 6h; Product distribution; also with coactivator and other activators, various times, reaction with other 2-phenoxyethanols;A n/a
B 53%
67-56-1

methanol

10113-28-7

dimethyl phenyl phosphate

124-41-4

sodium methylate

A

512-56-1

trimethyl phosphite

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 0℃; Rate constant;
at 19℃; Rate constant;
at 10℃; Rate constant;
60-29-7

diethyl ether

64-17-5

ethanol

13400-05-0

trichloro-methanesulfenic acid phenyl ester

141-52-6

sodium ethanolate

A

13029-05-5

trichloro-methanesulfenic acid ethyl ester

B

139-02-6

sodium phenoxide

64-17-5

ethanol

1247-19-4

diphenyldiphenoxysilane

furan-2,3,5(4H)-trione pyridine (1:1)

A

512-63-0

1,1,3,3,5,5-hexaphenylcyclotrisiloxane

B

139-02-6

sodium phenoxide

339199-98-3

1,3,5-trinitro-2,4,6-triphenoxy-benzene

141-52-6

sodium ethanolate

A

68959-41-1

1,3,5-triethoxy-2,4,6-trinitrobenzene

B

139-02-6

sodium phenoxide

110-54-3

hexane

676-54-0

ethyl sodium

100-66-3

methoxybenzene

139-02-6

sodium phenoxide

1247-19-4

diphenyldiphenoxysilane

furan-2,3,5(4H)-trione pyridine (1:1)

67-64-1

acetone

A

512-63-0

1,1,3,3,5,5-hexaphenylcyclotrisiloxane

B

139-02-6

sodium phenoxide

110-54-3

hexane

676-54-0

ethyl sodium

103-73-1

Phenetole

139-02-6

sodium phenoxide

623-11-0

1-methyl-4-nitrosobenzene

98-11-3

benzenesulfonic acid

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 310 - 360℃; Rate constant;
70310-90-6

N,N'-bis(diphenyloxyphosphonyl)-8-quinolinesulfinamidine

A

139-02-6

sodium phenoxide

B

64326-13-2

sodium naphthalene-1-sulfinate

Conditions
ConditionsYield
With sodium hydroxide for 3h; Product distribution; Heating;
93-99-2

benzoic acid phenyl ester

A

532-32-1

sodium benzoate

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane; water at 15℃; Rate constant; Thermodynamic data; Kinetics; var. temperatures, var. ratio of solvents, log A, Ea;
2122-46-5, 55748-05-5

phenoxy radical

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With Sodium borate; sodium azide; oxygen; sodium formate In water Rate constant; Irradiation; combination with superoxid anion radicals;
20376-70-9

phenyl N-methyl-N-m-nitrophenylcarbamate

A

619-26-1

N-methyl-3-nitroaniline

B

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium hydroxide; cetyltrimethylammonim bromide In methanol; water at 68.5℃; Rate constant; Mechanism; other N-methyl-N-arylcarbamates; reaction in absence of cetyltrimethylammonium bromide;
50882-34-3

Methyl-(4-nitro-phenyl)-carbamic acid phenyl ester

A

139-02-6

sodium phenoxide

B

100-15-2

N-methyl(p-nitroaniline)

Conditions
ConditionsYield
With sodium hydroxide; cetyltrimethylammonim bromide In methanol; water at 68.5℃; Rate constant;
3229-70-7

phenolate

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium cation In water; dimethyl sulfoxide at 25℃; Equilibrium constant;
3046-27-3

sodium m-chlorophenoxide

139-02-6

sodium phenoxide

Conditions
ConditionsYield
With sodium tetrahydroborate; hydrogen; PdCl2 complex on modified silca gel In methanol at 20℃; under 760 Torr; Rate constant; hydrogenolysis of chlorobenzenes in the presence of palladium chloride complex deposited on modified silica gel; effect of the nature of substituents in aromatic ring;
30616-32-1

1-phenylcarbamoyl-1-methylhydrazine

A

139-02-6

sodium phenoxide

B

C2H5N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; enegy parameters calculated from kobs in range 25-60 deg C; pH range 12.7, 13.9;
18197-54-1

N',N'-Dimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C3H7N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 12.0, 14.9;

N,N'-Dimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C3H7N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 13.0, 13.9;

N,N',N'-Trimethyl-hydrazinecarboxylic acid phenyl ester

A

139-02-6

sodium phenoxide

B

C4H9N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Mechanism; Thermodynamic data; energy parameters calculated from kobs in range 25-60 deg C; pH range 13.6, 14.1;
20605-43-0

phenyl hydrazinecarboxylate

A

139-02-6

sodium phenoxide

B

CH3N2O2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydroxide In methanol; water at 25℃; Rate constant; Thermodynamic data; Mechanism; energy parameters calculated from kobs in range 25-60 deg C; pH range 11.9, 14.9;
100-66-3

methoxybenzene

aqueous NaOH

aqueous NaOH

139-02-6

sodium phenoxide

Conditions
ConditionsYield
at 250 - 260℃;
110-86-1

pyridine

100-66-3

methoxybenzene

sodium

sodium

139-02-6

sodium phenoxide

60-29-7

diethyl ether

7664-41-7

ammonia

100-66-3

methoxybenzene

sodium

sodium

139-02-6

sodium phenoxide

60-29-7

diethyl ether

sodium amide

122-79-2

Phenyl acetate

A

60-35-5

acetamide

B

139-02-6

sodium phenoxide

sodium amide

122-79-2

Phenyl acetate

71-43-2

benzene

A

60-35-5

acetamide

B

139-02-6

sodium phenoxide

142-82-5

n-heptane

1822-71-5

n-pentylsodium

103-73-1

Phenetole

A

139-02-6

sodium phenoxide

B

2-ethoxy-phenyl sodium

2-ethoxy-phenyl sodium

Conditions
ConditionsYield
at 35℃; Product distribution;
at 75℃; Product distribution;
111-83-1

1-bromo-octane

139-02-6

sodium phenoxide

1818-07-1

octyloxybenzene

Conditions
ConditionsYield
poly<1-hydroxyethylene-co-1-(2-ethylsulf In 1,4-dioxane at 75℃; for 23h; Product distribution; Rate constant; other catalysts;100%
Sucrose-ethyleneoxide adducts In toluene at 110℃; for 8h; Product distribution; further catalysts: PEG, DB18K6; further objects of study: phase-transfer catalysis;100%
dodecyldimethylsulfonium methyl sulfate In water at 40℃; for 6h;25%
623-00-7

4-bromobenzenecarbonitrile

139-02-6

sodium phenoxide

3096-81-9

4-phenoxybenzonitrile

Conditions
ConditionsYield
With potassium phosphate In tetrahydrofuran at 115℃; for 18h;100%
With CF3-DPPF; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 20h;79.6%
With CF3-DPPF ligand; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran; toluene at 120℃; for 30h; Product distribution; various DPPF ligands for the Pd-catalyzed formation of diaryl ethers;
139-02-6

sodium phenoxide

13790-39-1

6,7-dimethoxy-4-chloroquinazoline

1180653-47-7

6,7-dimethoxy-4-phenoxyquinazoline

Conditions
ConditionsYield
In dimethyl sulfoxide at 80℃; for 3h;100%
3360-41-6

4-phenyl-butan-1-ol

139-02-6

sodium phenoxide

358349-92-5

(4-phenoxybutyl)benzene

Conditions
ConditionsYield
Stage #1: 4-phenyl-butan-1-ol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere;
Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere;
100%
31643-49-9

4-Nitrophthalonitrile

139-02-6

sodium phenoxide

38791-62-7

4-phenoxyphthalonitrile

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 1h;99%
1623-05-8

perfluoro(propyl vinyl ether)

139-02-6

sodium phenoxide

144373-62-6

(2-Chloro-1,1,2-trifluoro-2-heptafluoropropyloxy-ethoxy)-benzene

Conditions
ConditionsYield
With hexachloroethane In N,N-dimethyl-formamide 1) 25 deg C - 29 deg C, 2) r.t., overnight;99%
41663-84-7

4-nitro-N-methyl-phthalimide

139-02-6

sodium phenoxide

63197-24-0

4-phenoxy-N-methyl phthalimide

Conditions
ConditionsYield
N-neopentyl chloride of 4-dibutylaminopyridine In toluene at 110℃; for 1h;99%
In dimethyl sulfoxide at 15 - 120℃; for 24h; Inert atmosphere;93%

dimethyl-3-sulfopropyl(ferrocenylmethyl)ammonium

139-02-6

sodium phenoxide

hydroxymethylferrocene ethyl ether

Conditions
ConditionsYield
In water a mixt. of Fe compd. and C6H5ONa in water is refluxed for 5 min; mixt. is cooled and extd. with ether, extract is washed with ether and dried with sodium sulfate, removal of ether by distillation, recrystn. from heptane;99%
139-02-6

sodium phenoxide

83-01-2

diphenylcarbamic chloride

5416-45-5

diphenyl-carbamic acid phenyl ester

Conditions
ConditionsYield
at 20℃; for 0.08h; Neat (no solvent); Microwave irradiation; Grinding;99%
1610679-61-2

tert-butyl (3-bromo-5-chloropyrazolo[1,5-a]pyrimidin-7-yl)(2-morpholinoethyl)carbamate

139-02-6

sodium phenoxide

1610680-02-8

tert-butyl (3-bromo-5-phenoxypyrazolo[1,5-a]pyrimidin-7-yl)(2-morpholinoethyl)carbamate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 0.5h;99%
79696-96-1

2-Amino-6-chlor-3,4,5-pyridintricarbonitril

139-02-6

sodium phenoxide

2-Amino-6-phenoxy-3,4,5-tricyanopyridin

Conditions
ConditionsYield
In acetone for 0.5h; Heating;98%
139-02-6

sodium phenoxide

4-chloro-3-methylbut-2-enal dimethylacetal

1,1-dimethoxy-3-methyl-4-phenoxybut-2-ene

Conditions
ConditionsYield
In tetrahydrofuran; water for 48h; Ambient temperature;98%
139-02-6

sodium phenoxide

318956-66-0

C30H29Cl4N5O2P4S3

C54H49N5O6P4S3

Conditions
ConditionsYield
In tetrahydrofuran at 20℃;98%

C46H55NO5S

139-02-6

sodium phenoxide

C45H53NO3

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃;98%
139-02-6

sodium phenoxide

19579-04-5

tetrachlorophenoxyphosphorane

Conditions
ConditionsYield
With phosphorus pentachloride In tetrachloromethane at -15℃; for 1h;98%
3597-91-9

biphenyl-4-yl methanol

139-02-6

sodium phenoxide

29263-69-2

1-phenyl-4-phenoxymethylbenzene

Conditions
ConditionsYield
Stage #1: biphenyl-4-yl methanol With 1,2-Diiodoethane; N,N-dimethyl-formamide; triphenylphosphine at 20℃; for 0.0166667h; Sealed tube; Inert atmosphere;
Stage #2: sodium phenoxide at 20℃; Sealed tube; Inert atmosphere;
98%
100-67-4

potassium phenolate

139-02-6

sodium phenoxide

1184-10-7

2,2,4,4,6,6-hexaphenoxycyclotriphosphazene

Conditions
ConditionsYield
With cesium hydroxide; 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine In 1,2-dichloro-benzene at 175℃; Product distribution / selectivity;97.9%
139-02-6

sodium phenoxide

79-11-8

chloroacetic acid

108-95-2

phenol

122-59-8

2-phenoxyacetic acid

Conditions
ConditionsYield
at 105℃; pH=9 - 10;97.6%
139-02-6

sodium phenoxide

96-34-4

methyl chloroacetate

2065-23-8

methyl 2-phenoxyacetate

Conditions
ConditionsYield
at 120℃; for 6h; Temperature;97.5%
17455-13-9

18-crown-6 ether

139-02-6

sodium phenoxide

C12H24O6*3C6H5O(1-)*3Na(1+)

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 1h; Ambient temperature;97%
139-02-6

sodium phenoxide

350-46-9

4-Fluoronitrobenzene

620-88-2

4-nitrophenyl phenyl ether

Conditions
ConditionsYield
N-2-ethylhexyl chloride of 4(4-methylpiperidinyl)pyridine In toluene at 110℃; for 0.25h;97%
With ammonia at 25℃; Kinetics; Concentration;

(7-methoxy[2.2]paracyclophan-4-yl)(4'-methoxyphenyl)iodonium hexafluorophosphate

139-02-6

sodium phenoxide

A

1655-69-2

1-methoxy-4-phenoxy-benzene

B

1235887-94-1

4-methoxy-7-iodo[2.2]paracyclophane

Conditions
ConditionsYield
In [D3]acetonitrile at 80℃; for 1h; Inert atmosphere; Darkness; regioselective reaction;A 75%
B 97%
1313436-04-2

(S)-(1-benzyl-2,5-dihydro-1H-pyrrol-2-yl)methanol

139-02-6

sodium phenoxide

1313435-87-8

(R)-1-benzyl-3-phenoxy-1,2,3,6-tetrahydropyridine

Conditions
ConditionsYield
Stage #1: (S)-(1-benzyl-2,5-dihydro-1H-pyrrol-2-yl)methanol With trifluoromethylsulfonic anhydride In dichloromethane at -15℃; Inert atmosphere;
Stage #2: sodium phenoxide In tetrahydrofuran; dichloromethane at -15 - 20℃; Inert atmosphere; optical yield given as %ee; regioselective reaction;
97%

C29H36ClIrP2S2

139-02-6

sodium phenoxide

C35H41IrOP2S2

Conditions
ConditionsYield
In dichloromethane at 20℃; for 36h; Inert atmosphere; Glovebox;97%

4-(bromomethyl)-1,3-bis(2,6-diisopropylphenyl)-1,2,3-triazolium hexafluorophosphate

139-02-6

sodium phenoxide

1,3-bis(2,6-diisopropylphenyl)-4-(phenoxymethyl)-1,2,3-triazolium hexafluorophosphate

Conditions
ConditionsYield
In water; acetone at 20℃; for 12h; Schlenk technique;97%
1698-53-9

4,5-dichloro-1-phenylpyridazin-6-one

139-02-6

sodium phenoxide

38387-54-1

5-chloro-4-phenoxy-2-phenyl-2H-pyridazin-3-one

Conditions
ConditionsYield
In 1,4-dioxane for 16h; Ambient temperature;96%
64891-77-6

(2-13C)bromoacetic acid

139-02-6

sodium phenoxide

134757-64-5

<2-13C>-2-phenoxyacetic acid

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 2h; Heating;96%
60410-77-7

bis(4-methylbenzenethiocarbonyl) sulphide

139-02-6

sodium phenoxide

52322-79-9

O-phenyl 4-methylbenzenecarbothioate

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether; ethanol for 3h; Ambient temperature;96%
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    Sodium benzenolate CAS NO.139-02-6

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    Phenol, sodium salt(1:1)

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     China (Mainland)  |  Contact Details

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    Changsha EASCHEM is a leading company in marketing ang distributing chemicals and new materials with establishment in 2013 by reregistering from Easchem International from China. We, EASCHEM, are the brand with the aim for erecting up Big Chemica

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    Business Type:Manufacturers

    Tel:86-571-86465881,86-571-87157530,86-571-88025800

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    139-02-6

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    139-02-6

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    139-02-6

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    139-02-6

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Chemistry

Synonyms: PHENOL,sodiumsalt;PHENOL,sodiumsalt(solid);PHENOLatesodium;PHENOLsodium;PHENOLsodiumsalt;sodiumcarbolate;sodiumPHENOLate,solid;SODIUM PHENATE
SODIUM PHENOXIDE is the chemical compound with the formula C6H5NaO.Its molar mass is 116.09.
density:0,898 g/cm3
Flash point:28°C
storage temp.:below 5° C
Sensitive:Hygroscopic

Toxicity Data With Reference

1.   

scu-mus LDLo:350 mg/kg

   AEXPBL    Archiv fuer Experimentelle Pathologie und Pharmakologie. 52 (1905),220.
2.   

scu-frg LDLo:100 mg/kg

   AEXPBL    Archiv fuer Experimentelle Pathologie und Pharmakologie. 52 (1905),220.

Consensus Reports

Sodium PHENOXIDE's reported in EPA TSCA Inventory.

Safety Profile

Poison by subcutaneous route. A corrosive irritant to skin, eyes, and mucous membranes. When heated to decomposition it emits toxic fumes of Na2O. See also PHENOL and SODIUM HYDROXIDE.

Standards and Recommendations

DOT Classification:  8; Label: Corrosive