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593-81-7

Basic Information
CAS No.: 593-81-7
Name: Trimethylamine hydrochloride
Article Data: 62
Cas Database
Molecular Structure:
Molecular Structure of 593-81-7 (Trimethylamine hydrochloride)
Formula: C3H10ClN
Molecular Weight: 95.5721
Synonyms: Methanamine,N,N-dimethyl-, hydrochloride (9CI);Trimethylamine, hydrochloride (8CI);Trimethylamine hydrochloric acid;Trimethylamine monohydrochloride;Trimethylammonium chloride;
EINECS: 209-810-0
Density: 0.692g/cm3
Melting Point: 283-284 °C (dec.)(lit.)
Boiling Point: 2.8oC at 760 mmHg
Flash Point: N/A
Solubility: Soluble in water
Appearance: white to slightly cream crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36-37/39
Transport Information: N/A
PSA: 3.24000
LogP: 0.97980
Synthetic route
1184-78-7

trimethylamine-N-oxide

68-12-2, 33513-42-7

N,N-dimethyl-formamide

97-00-7

1-chloro-2,4-dinitro-benzene

A

51-28-5

2,4-Dinitrophenol

B

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
for 24h; Ambient temperature;A 97%
B 98%
1184-78-7

trimethylamine-N-oxide

97-00-7

1-chloro-2,4-dinitro-benzene

A

51-28-5

2,4-Dinitrophenol

B

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 24h; Ambient temperature;A 97%
B 98%
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-formamide dimethyl acetal With [1,4-bis(diphenylphosphino)butane](1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen In methanol at 25℃; under 30003 Torr; Autoclave;
Stage #2: With hydrogenchloride In methanol; water Reagent/catalyst;
96%
50-00-0

formaldehyd

124-40-3

dimethyl amine

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
With oxalic acid at 100 - 120℃; Eschweiler-Clarke methylation;84%
67-56-1

methanol

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
Stage #1: methanol With ammonium hydroxide; Ag/TiO2 at 25℃; for 10h; UV-irradiation;
Stage #2: With hydrogenchloride In water
80%
68-12-2, 33513-42-7

N,N-dimethyl-formamide

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; lithium borohydride; chloro-trimethyl-silane In tetrahydrofuran for 24h; Ambient temperature;72%
Stage #1: N,N-dimethyl-formamide With tris(bis(trimethylsilyl)amido)lanthanum(III); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In benzene at 25℃; for 1h; Inert atmosphere; Glovebox;
Stage #2: With hydrogenchloride In methanol at 0℃;
50%
Stage #1: N,N-dimethyl-formamide With tris((4,4-dimethyl-2-oxazolinyl)phenylborate) MgMe; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Stage #2: With hydrogenchloride
18%
146475-62-9

cyclopropanesulfonyl-1-d chloride

67-63-0

isopropyl alcohol

75-50-3

trimethylamine

A

593-81-7

trimethylamine hydrochloride

B

146475-51-6

propan-2-yl cyclopropanesulfonate

C

N,N-dimethylcyclopropanesulfonamide-1-d

Conditions
ConditionsYield
In dichloromethane at 25℃; for 36h;A n/a
B 11.7%
C 27.4%
88470-26-2

N,N-dimethoxyamine

75-50-3

trimethylamine

A

593-81-7

trimethylamine hydrochloride

B

75-57-0

tetramethlyammonium chloride

Conditions
ConditionsYield
With tert-butylhypochlorite In diethyl ether 1) -78 deg C, 0.5 h, 2) -8 deg C, 24 h;A 15.7%
B 22.8%

Cl2B-N(CH3)2*N(CH3)3

999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

A

32882-72-7

Bis(trimethylsilyl)aminochlorodimethylaminoboran

B

593-81-7

trimethylamine hydrochloride

Conditions
ConditionsYield
In benzene stirring for 1 week in dry benzene; sepn. of trimethylamine hydrochloride and benzene;A 16%
B n/a
In benzene stirring for 1 week in dry benzene; sepn. of trimethylamine hydrochloride and benzene;A 16%
B n/a
108-88-3

toluene

6001-87-2

methyl 3-chloropropionate

75-50-3

trimethylamine

A

593-81-7

trimethylamine hydrochloride

B

16332-33-5

(2-methoxycarbonylethyl)trimethylammonium chloride

Conditions
ConditionsYield
at -5℃;
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Chemistry

Molecular structure of Trimethylamine hydrochloride (CAS NO.593-81-7) is:

Product Name: Trimethylamine hydrochloride
CAS Registry Number: 593-81-7
IUPAC Name: N,N-dimethylmethanamine hydrochloride
Molecular Weight: 95.5712 [g/mol]
Molecular Formula: C3H10ClN
H-Bond Donor: 1
H-Bond Acceptor: 1 
EINECS: 209-810-0
Melting Point: 283-284 °C (dec.)(lit.)
Storage temp.: 2-8°C
Water Solubility: Soluble
Sensitive: Hygroscopic
Enthalpy of Vaporization: 22.94 kJ/mol
Boiling Point: 2.8 °C at 760 mmHg
Vapour Pressure: 1720 mmHg at 25°C

Uses

 Trimethylamine hydrochloride (CAS NO.593-81-7) is used as a raw material of choline chloride, ion exchange resins, tetramethyl ammonium hydroxide, oil field chemicals, quaternary ammonium compounds, cationic starch reagents, phase transfer catalyst, pesticides as well as a warning agent for natural gas and flotation agent.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intravenous 325mg/kg (325mg/kg)   Medicina et Pharmacologia Experimentalis. Vol. 16, Pg. 529, 1967.

Safety Profile

Hazard Codes: IrritantXi
Risk Statements: 36/37/38 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36-37/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36:Wear suitable protective clothing. 
S37/39:Wear suitable gloves and eye/face protection.
WGK Germany: 1
RTECS: YH2700000
F: 3-10
HS Code: 29211190

Specification

 Trimethylamine hydrochloride , its cas register number is 593-81-7. It also can be called Trimethylammonium chloride ; Methanamine, N,N-dimethyl-, hydrochloride .It is a white to slightly cream crystalline powder.