Hydrolysis of aromatic nitriles using 20% aqueous KOH (CAS 1310-58-3)
Sintered silicon carbide: A new ceramic vessel material for microwave chemistry in single-mode reactors
Scheme 7
Not unlike ionic liquids, the distinctly polar properties of TREAT-HF make it very suitable as a reagent (and/or solvent) in microwave-heated transformations. In fluorine– chlorine exchange reactions involving (trichloromethylthio)-benzene at 250℃ (Scheme 6)[36] we did, however, notice a significant corrosion of standard Pyrex microwave reaction vials in the vapor space above the liquidꢃs surface.
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