2648-61-5Relevant articles and documents
γ-Alkylthio-γ-chloro-α,β-dicarbonyl Compounds
Guseinov,Burangulova,Ismailov
, p. 742 - 743 (2003)
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Jackson
, p. 977 (1934)
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Method for synthesizing mandelic acid
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Paragraph 0032-0033; 0035-0036; 0038-0039; 0041-0042, (2021/02/06)
The invention relates to the technical field of compound preparation, and provides a method for synthesizing mandelic acid, which comprises the following steps: by using styrene as a basic raw material, trichloroisocyanuric acid as a chlorinating agent an
Solvent-free preparation of α,α-dichloroketones with sulfuryl chloride
Tu, Dewei,Luo, Juan,Jiang, Wengao,Tang, Qiang
supporting information, (2021/09/15)
An efficient and facile method is reported for the synthesis of a series of α,α-dichloroketones. The direct dichlorination of methyl ketones and 1,3-dicarbonyls using an excess amount of sulfuryl chloride affords the corresponding gem-dichloro compounds in moderate to excellent yields. Moreover, the protocol features high yields, broad substrate scope, and simple reaction conditions without using any catalysts and solvents.