Synthesis p. 139 - 140 (1986)
Update date:2022-08-04
Topics:
Ando, Wataru
Takata, Toshikazu
Huang, Liren
Tamura, Yoshiharu
3-Methyl 1,3-thiazolidines 3a-c can be prepared easily in good yields by the reaction of β-mercaptoamine derivatives 1a-c with formalin and formic acid in a one-pot operation.The same procedure is also suitable for the construction of the 3-methyl-tetrahydro-1,3-thiazine skeleton from γ-mercaptoamines as exemplified in the synthesis of 3d.
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Doi:10.1016/j.bmcl.2008.05.092
(2008)Doi:10.1021/ja00963a032
(1966)Doi:10.1021/jo00094a033
(1994)Doi:10.1248/cpb.35.2594
(1987)Doi:10.1021/ja01173a068
(1949)Doi:10.1248/cpb.40.2707
(1992)
