
Journal of Organic Chemistry p. 2760 - 2762 (1987)
Update date:2022-08-05
Topics:
Raucher, Stanley
Gustavson, Linda M.
Stencamp, Ronald E.
Treatment of the homoallyl oxyacetic acid 7 with excess LDA at -78 deg C followed by thermolysis at 185 deg C in HMPA provided the unusual cyclization product 8a.A single-crystal X-ray structure was obtined for the derivative 8c.
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