Tetrahedron Letters p. 5025 - 5028 (1986)
Update date:2022-09-26
Topics:
Moloney, Mark G.
Pinhey, John T.
Roche, Eric G.
The addition of lead tetraacetate to a chloroform solution of alk-1-ynyltrimethylstannane results in the rapid formation of trimethylstannyl acetate and an unstable species, believed to be the corresponding alk-1-ynyllead triacetate, which can effect the rapid α-alkynylation of β-dicarbonyl compounds and nitronate salts.
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Doi:10.1021/acs.jmedchem.6b00726
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