Tetrahedron Letters p. 6891 - 6894 (1995)
Update date:2022-07-31
Topics: Reagent Chemoselective Desilylation Experimental Chemical tert-butyldimethylsilyl ethers
Lee, Adam Shih-Yuan
Yeh, Hsiu-Chih
Tsai, Ming-Hung
The use of a 0.25M CH3OH/CCl4 (1:1) solvent mixture under ultrasound for the selective deprotection of tert-butyldimethylsilyl ethers of benzyl alcohols is described.This method enables to deprotect tert-butyldimethylsilyl ethers of primary alcohols, whereas tert-butyldimethylsilyl ethers of secondery and tertiary alcohols were stable under the reaction condition.
View Morewebsite:http://www.np-chem.com
Contact:0086-25-52346877
Address:199, Jian Ye Road, Nanjing, China
Lianyungang Ningkang Chemical Co., Ltd
Contact:.+86-518-88588008
Address:http://www.chemnk.com
Contact:+86-021-50792271
Address:Building 24A, 300 Chuantu Road, Chuansha, Pudong new area, Shanghai, China, 201202
Contact:+86-574-89075960
Address:#100 Xiang Yun Road, New High tech area, Ningbo, China
Ningbo Tide Imp. & Exp. Co., Ltd.
Contact:+86-571-8993 7933; +86-571-8993 6453
Address:7/F Anno Domini Building, Tower South, 8 Qiu Shi Road,Hangzhou,China.
Doi:10.1039/jr9580001367
(1958)Doi:10.1039/jr9560004422
(1956)Doi:10.1039/c2ra22115b
(2013)Doi:10.1016/j.tet.2007.06.014
(2007)Doi:10.1016/S0020-1693(00)83911-0
(1988)Doi:10.1055/s-0034-1379207
(2015)
