Steroids p. 395 - 400 (1986)
Update date:2022-08-03
Topics:
Leon
Mettler
Hylarides
The preparation of 6 beta-methoxy-7 alpha-bromoestradiol (1) is reported. Addition of in situ-generated BrOMe to 6-dehydroestradiol 3-tetrahydropyranyl ether (4a) afforded the expected addition product. Removal of the tetrahydropyranyl protective group was carried out by mild acid hydrolysis to afford 1 in good yields. This base-sensitive compound is chemically stable over long periods of time.
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Doi:10.1248/cpb.35.4562
(1987)Doi:10.1016/j.steroids.2010.05.017
(2010)Doi:10.1016/j.jorganchem.2008.11.029
(2009)Doi:10.1039/b822955d
(2009)Doi:10.1002/chem.200802626
(2009)Doi:10.1021/jo034593i
(2003)
