
Synthetic Communications p. 1371 - 1376 (2010)
Update date:2022-07-29
Topics:
Zhu, Min
Cai, Cheng Gang
Ke, Wei
Shao, Jing
A convenient, solvent-free method for preparation of [hydroxy(phosphoryloxy)iodo]arenes is reported. (Diacetoxyiodo)benzene or other hypervalent iodine reagents and phosphates are simply blended and ground for several minutes in an agate mortar, giving good yields of [hydroxy(phosphoryloxy)iodo]arenes with excellent purities.
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