Tetrahedron Letters p. 1225 - 1228 (1989)
Update date:2022-08-02
Topics:
Haider, Karl
Soundararajan, N.
Shaffer, Myron
Platz, Matthew S.
Photolysis of 2,4,6-trifluoro-1,3-diazidobenzene in 2-methyltetrahydrofuran at 77k produces a dinitrene quintet.Upon warming the quintet briefly to 100K followed by recooling to 77K the EPR spectrum of the quintet disappears and is replaced by that of a trifluorodiaza biradical.
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Doi:10.1021/acs.orglett.6b01515
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