A controlled synthesis of α-(E)-1-alkenyl ketones from β-keto benzyl esters

DOI: 10.1016/S0040-4039(01)93932-2

Source and publish data:

Tetrahedron Letters p. 7195 - 7198 (1989)

Update date:2022-08-03

Topics: Characterization Deprotection Purification and Isolation Protection of the Carbonyl Group

Authors:

Hashimoto

Miyazaki

Shinoda Shinoda

Ikegami Ikegami

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Article abstract of DOI:10.1016/S0040-4039(01)93932-2

A regio- and stereocontrolled method for the synthesis of α-(E)-1-alkenyl ketones from β-keto benzyl esters has been developed by devising the sequence of a modified Pinhey's alkenylation and a reductive removal of a benzyloxycarbonyl group with Raney nic

Full text of DOI:10.1016/S0040-4039(01)93932-2

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Product name:1-[(E)-3-(tert-Butyl-dimethyl-silanyloxy)-propenyl]-3-methyl-2-oxo-cyclohexanecarboxylic acid benzyl ester

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