CHIRALE INDUKTION BEI DER PHOTOCHEMISCHEN UMLAGERUNG VON 3,6-HEXANOOXEPIN-4,5-DICARBONSAEUREESTERN

DOI: 10.1016/S0040-4039(01)93370-2

Source and publish data:

Tetrahedron Letters p. 6855 - 6858 (1989)

Update date:2022-08-04

Topics:

Authors:

Tochtermann, Werner

Schloesser, Ulrike

Popp, Brigitta

Peters, Eva-Maria

Peters, Karl

Schnering, Hans Georg von

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Article abstract of DOI:10.1016/S0040-4039(01)93370-2

Irradiation of an aqueous suspension of the crystalline diester 1d affords the (+)-(3aS, 6R, 8aR)-methanohydroazulene 2d in 45percent yield with 83percent de.The absolute configurations were established via the X-ray structural analysis of the dimenthylester (+)-2b and chemical transformations.

Full text of DOI:10.1016/S0040-4039(01)93370-2

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