Journal of Coordination Chemistry p. 3926 - 3938 (2013)
Update date:2022-09-26
Topics:
Chai, Lan-Qin
Liu, Gang
Zhang, Yu-Li
Huang, Jiao-Jiao
Tong, Jun-Feng
An unexpected mononuclear Ni(II) complex, [Ni(L2) 2]·CH3OH (HL2 = 1-(2-{[(E)-3,5-dichloro- 2-hydroxybenzylidene]amino}phenyl)ethanone oxime), has been synthesized via complexation of Ni(II) acetate tetrahydrate with HL1. HL1 and its corresponding Ni(II) complex were characterized by IR, 1H-NMR spectra, HRMS, as well as by elemental analysis, UV-vis, and emission spectroscopy. The crystal structure of the complex has been determined by single-crystal X-ray diffraction. Each complex links two other molecules into an infinite 1-D chain via intermolecular hydrogen bonds. Moreover, the electrochemical properties of the nickel complex were studied by cyclic voltammetry. Superoxide dismutase-like activities of HL1 and Ni(II) complex were also investigated.
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