Journal of Organic Chemistry p. 6025 - 6031 (1992)
Update date:2022-08-04
Topics:
Pettersson, Helena
Gogoll, Adolf
Baeckvall, Jan-E.
Epoxidation of syn- and anti-5-(tosylamido)-3-hexen-2-ol derivatives was studied using three different epoxidation reagents: (i) m-CPBA, (ii) t-BuOOH/VO(acac)2, and (iii) t-BuOOH/Ti(O-i-Pr)4.A method for the stereochemical assignment of the 3,4-epoxy-5-(tosylamido)-3-hexen-2-ol derivatives obtained was developed by the use of NMR spectroscopy.
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