
Bulletin of the Chemical Society of Japan p. 3828 - 3830 (1993)
Update date:2022-08-02
Topics:
Okada
Ishii
Nishimura
Dimethoxy[n.2]metacyclophanes were obtained in 5 45% yields through [2+2] photocycloaddition of corresponding styrene derivatives. These cyclobutane- fused metacyclophanes were assigned to be of only syn conformation (n = 6, 8, 10, and 12). The cyclobutane ring exclusively tool the opposite direction to the alkyl bridged chain.
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