Intra-annular reactions of the (1,3-xylylene)-18-crown-5 system: synthesis and crystal structure of -18-crown-5, -18-crown-5 and bismercury

DOI: 10.1016/0022-328X(93)83392-9

Source and publish data:

Journal of Organometallic Chemistry p. 7 - 22 (1993)

Update date:2022-08-02

Topics:

Authors:

Markies, Peter R.

Villena, Alan

Akkerman, Otto S.

Bickelhaupt, Friedrich

Smeets, Wilberth J. J.

Spek, Anthony L.

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Article abstract of DOI:10.1016/0022-328X(93)83392-9

The Grignard compound <2-(bromomagnesio)-1,3-xylylene>-18-crown-5 (4) was prepared from the aryllithium compound (2-lithio-1,3-xylylene)-18-crown-5 (9) and magnesium bromide.The crystal structure of 4 shows that it crystallizes without solvent and is coor

Full text of DOI:10.1016/0022-328X(93)83392-9

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