Tetrahedron p. 3525 - 3534 (1995)
Update date:2022-07-29
Topics:
Gormanns, Marcus
Ritter, Helmut
Polymerizable N-methacrylamino m-BOC-type, 1,1-dimethyl-2-methacrylmethanamido-ethoxy-carbonyl- and 1,1-dimethyl-3-methacrylmethanamido-butoxy-carbonyl group, derived from the corresponding t-alcohols have been developed as acid labile aminoprotecting groups. The synthesis of monomeric and polymeric N-methacrylamino m-BOC amino acids and amino acid methyl esters and their application for peptide synthesis following the (N→C)-assembly method are described. The rapid, acid induced cleavage of the protecting group leads to the formation of oxazole resp. oxazine derivatives.
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Doi:10.1007/BF00809947
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