Chemical Communications p. 2621 - 2622 (1996)
Update date:2022-08-02
Topics:
Chaubon, Marie-Anne
Escudie, Jean
Ranaivonjatovo, Henri
Satge, Jacques
The dimesityl(diisitylstanna)germene 4 [isityl (Is) = 2,4,6-triisopropylphenyl] is synthesized by dehydrofluorination of the corresponding (fluorostannyl)germane 1 by tert-butyllithium at low temperature; its structure is evidenced at -20°C by 119Sn NMR spectroscopy (δ + 360), by addition of water and methanol to the tin-germanium double bond and by a [2 + 2] cycloaddition with benzaldehyde; warming the stannagermene 4 to room temperature affords the dimesityl(tetraisityldistanna)germirane 8.
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Doi:10.1007/BF00810292
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