Hydrazinium heptafluorouranate(V). Preparation, properties, and thermal decomposition

Article abstract of DOI:10.1021/ic50038a010

The new compound, hydrazinium heptafluorouranate(V), was prepared at 0° by the reaction of hydrazinium difluoride and uranium hexafluoride both in anhydrous hydrogen fluoride and in carbon tetrachloride. The magnetic moment of the yellowish compound at 0° is 1.66 BM. X-Ray powder diffraction data are given. The thermal decomposition of the compound in an inert atmosphere proceeds as follows: (Chemical Equation Presented) A detailed discussion of this thermal decomposition is given.