Nucleosides and Nucleotides p. 417 - 432 (1997)
Update date:2022-08-05
Topics:
Daily
Schwartz
Riley
Arnold L.J.
Marvin
Scurria
Hopkins
Atkins
Garcia
Pirrung
A diastereoselective dinucleoside methylphosphonate synthetic method that features coupling of diastereomerically pure 1,1,1,3,3,3-hexafluoro-2- propyl nucleoside-3'-O-methylphosphonate monomers with 3'-O-protected nucleoside monomers mediated by alkoxymagnesium chloride reagents is described. This synthetic method was found to be diastereospecific in the synthesis of selected 2'-deoxy dinucleoside methyphosphonates and diastereoselective in the synthesis of all sixteen 2'-O-methyl dinucleoside methylphosphonates.
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Doi:10.1139/v61-319
(1961)Doi:10.1016/S0040-4020(97)90398-7
(1997)Doi:10.1021/jo9700787
(1997)Doi:10.1016/S0022-328X(96)06890-8
(1997)Doi:10.1016/S0022-328X(96)06906-9
(1997)Doi:10.1016/S0223-5234(97)89090-3
(1997)