Organic and Biomolecular Chemistry p. 7959 - 7963 (2018)
Update date:2022-07-30
Topics:
Zhou, Bang
Chen, Wenqi
Yang, Yuzhong
Yang, Yuan
Deng, Guobo
Liang, Yun
A convenient radical cyclization cascade procedure for the construction of sulfonated indenones from 2-alkynylbenzonitriles and sodium arylsulfinates has been explored under mild reaction conditions. The present methodology offers a low-cost and operationally straightforward approach to synthesizing various sulfonated indenones in moderate to good yields by simple use of cheap sodium persulfate as an oxidant and environmentally benign water as a co-solvent.
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