Tetrahedron Letters p. 8589 - 8592 (1998)
Update date:2022-08-04
Topics: Regioselectivity Yield NMR spectroscopy Stereochemistry Chromatography Mass spectrometry (MS) PHOTOCHEMICAL REACTION Alkene Intermediate Aromatic ring Retrosynthetic analysis Cycloaddition Reaction Optimization Photocycloaddition Synthetic Strategy Natural product Formal Synthesis
Wender, Paul A.
Dore, Timothy M.
Starting from triethyl phosphonopropionate and 3-nitro-2-methylbenzoic acid, a formal synthesis of crinipellin B was achieved. The strategy draws on the use of a novel version of the arene-alkene meta-photocycloaddition reaction that proceeds with the generation of 4 rings and 4 quaternary stereocenters in one synthetic operation.
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Doi:10.1055/s-0036-1591566
(2018)Doi:10.1021/om980823l
(1998)Doi:10.1016/S0960-894X(98)00613-1
(1998)Doi:10.1021/ic9909072
(1999)Doi:10.1039/a807975g
(1998)Doi:10.1016/S0022-1139(98)00267-X
(1998)
