Chemistry Letters p. 567 - 568 (1999)
Update date:2022-07-30
Topics:
Kamijo, Kazunori
Toyota, Kozo
Yoshifuji, Masaaki
A stabilized thioxophosphine bearing the 2,4-di-t-butyl-6-(methylthiomethyl)phenyl group was generated either by reaction of the corresponding phosphonous dichloride with bis(trimethylsilyl) sulfide or by desulfurization reaction of the corresponding dithioxophosphorane using tris(dimethyl-amino)phosphine. The thioxophosphine, thus generated was trimerized to trithiatriphosphinane.
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