Synthetic Communications p. 319 - 328 (2002)
Update date:2022-07-30
Topics:
Amssoms
Augustyns
Yamani
Zhang
Haemers
A major problem in the use of spermidine for the synthesis of biologically interesting compounds is the selective orthogonal protection of the three different amino groups. Our approach is based on the Fukuyama reaction, starting from putrescine and 3-amino-l-propanol and affording N8-benzyloxycarbonyl- N1-tert-butyloxycarbonyl- N4-(2-nitrobenzenesulfonyl)spermidine (5) in 5 steps in high yield.
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