Journal of the Chemical Society. Perkin transactions I p. 2615 - 2619 (1981)
Update date:2022-07-30
Topics:
Atkinson, Robert S.
Judkins, Brian D.
Oxidation of 2,4-dinitrobenzenesulphenamide with lead tetra-acetate in the presence of electron-rich alkenes (styrene, (E)- and (Z)-1-phenylpropene, 2-phenylpropene, (Z)-but-2-ene, and butadiene) gives the corresponding substituted N-(2,4-dinitrophenylsulphenyl))aziridines.Intermolecular trapping of a presumed sulphenylnitrene intermediate is also successful in the oxidation of 2-nitrobenzenesulphenamide but fails for RSNH2 when R = PhCO, 4-ClC6H4, or 4-NO2C6H4.
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Doi:10.1039/c39840000735
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