Journal of Organic Chemistry p. 8674 - 8682 (2019)
Update date:2022-08-03
Topics:
Hokamp, Tobias
Wirth, Thomas
A novel class of chiral hypervalent iodine reagents containing an α-tetralol scaffold is introduced. Iodine triacetate is employed in a key step as a highly selective and efficient iodinating reagent for a short and convenient synthesis of iodine(III) derivatives. Solid-state X-ray analyses offer valuable structural information, while reactivities and stereoselectivities are investigated in three model reactions.
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