Journal of Organic Chemistry p. 555 - 560 (1982)
Update date:2022-09-26
Topics:
Still, Ian W. J.
Kutney, Gerald W.
McLean, David
The reaction of various aromatic and suitably substituted aliphatic thiones with sulfur dichloride in dry carbon disulfide affords the corresponding α-chlorothiosulfenyl chlorides (R2C(Cl)SSCl), the first simple compounds of this type.Reaction of the α-chlorothiosulfenyl chlorides with triphenylphosphine regenerates the thiones, accompanied by the corresponding ketones.Possible mechanisms for these transformations are presented.
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