Journal of the Chemical Society. Chemical communications p. 477 - 478 (1983)
Update date:2022-08-11
Topics:
King, R. Bruce
Sadanani, Narayan D.
Sundaram, Ponnuswamy M.
Reduction of (iPr2N)2PCl with LiAlH4 in diethyl ether gives (iPr2N)2PH; reaction of iPr2NPCl2 with Mg in boiling tetrahydrofuran gives either the cyclotetraphosphine (iPr2N)4P4 or the 1,2-dichlorobiphosphine iPr2NP(Cl)-P(Cl)NiPr2 depending upon the Mg:iPr2NPCl2 mole ratio.
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