New Journal of Chemistry p. 526 - 529 (2021)
Update date:2022-08-11
Topics:
Lu, Tian
He, Yuna
Song, Jia
Hou, Zhengwen
Yin, Hongquan
Fan, Guijuan
Chen, Fu-Xue
Eight energetic salts with a gem-dinitro group based on 1,2,4-oxadiazole were developed. All of the structures were confirmed by infrared (IR) spectroscopy, 1H and 13C nuclear magnetic resonance (NMR) spectroscopy, and high-resolution mass spectrometry (HRMS), and single-crystal X-ray diffraction was used to determine the structures of the pivotal intermediate 3-(chlorodinitromethyl)-5-methyl-1,2,4-oxadiazole (3), the potassium salt (4) and the hydrazinium salt (7). All of them are insensitive to impact (>40 J) and have higher energy levels than trinitrotoluene (TNT). This journal is
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