Chemistry of Heterocyclic Compounds p. 313 - 315 (1980)
Update date:2022-08-11
Topics:
Ermakova, T.G.
Gritsa, A.I.
Deriglazov, N.M.
Tatarova, L.A.
Keiko, V.V.
et al.
The polarographic reduction of 1-substituted 1,2,4-triazoles in dimethylformamide (DMF) and acetonitrile was studied. 1-Methyl-, 1-ethyl-, and 1,2,4-triazoles are not reduced on a mercury electrode over the range of potentials accesible for polarography. 1-Phenyl-1,2,4-triazole and 1-vinyl-1,2,4-triazole are reduced in acetonitrile via a one-electron mechanism at high negative potentials.The reduction of 1-vinyl-1,2,4-triazole is accompanied by polymerization of the electrolysis products.A possible mechanism for the electrochemical reduction is discussed.
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