CHLOROFLUOROACETYL FLUORIDE

Base Information

• Chemical Name: CHLOROFLUOROACETYL FLUORIDE
• CAS No.: 359-34-2
• Molecular Formula: C2H Cl F2 O
• Molecular Weight: 114.479
• Hs Code.: 2915900090
• Mol file: 359-34-2.mol

Synonyms:Acetylfluoride, chlorofluoro- (8CI,9CI)

Chemical Property of CHLOROFLUOROACETYL FLUORIDE

Chemical Property:

• Vapor Pressure: 28.5mmHg at 25°C
• Refractive Index: 1.327
• Boiling Point: 106.3°Cat760mmHg
• Flash Point: 18.1°C
• PSA: 17.07000
• Density: 1.407g/cm³
• LogP: 1.01690

Purity/Quality:

98%min ^*data from raw suppliers

CHLOROFLUOROACETYL FLUORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 34-36/37/38
• Safety Statements: 23-26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHLOROFLUOROACETYL FLUORIDE

There total 5 articles about CHLOROFLUOROACETYL FLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.5%

ethoxyflurane (310-71-4) → 1-fluoroethane (353-36-6) + chloroethane (75-00-3) + chlorofluoroacetyl fluoride (359-34-2) + chlorofluoroacetyl chloride (359-32-0)

Guidance literature:

With aluminium trichloride; for 1.58333h;

DOI:10.1016/S0022-1139(00)82333-7

Reference yield: 45.4%

ethoxyflurane (310-71-4) → 1-fluoroethane (353-36-6) + chlorofluoroacetyl fluoride (359-34-2)

Guidance literature:

With boron trifluoride diethyl etherate; for 16.75h; Heating; var. reag.: AlCl₃;

DOI:10.1016/S0022-1139(00)82333-7

Reference yield:

aluminium trichloride (7446-70-0) + 2-chloro-1,1,2-trifluoroethyl methyl ether (425-87-6) → methylene chloride (74-87-3) + Methyl fluoride (593-53-3) + chlorofluoroacetyl fluoride (359-34-2)

Guidance literature:

DOI:10.1021/ja01634a073 DOI:10.1021/ja01123a048

upstream raw materials:

ethoxyflurane

benzyl 2-chloro-1,1,2-trifluoroethyl ether

aluminium trichloride

2-chloro-1,1,2-trifluoroethyl methyl ether

Downstream raw materials:

ethyl chlorofluoroacetate

2-chloro-2-fluoro-N-phenylacetamide

Refernces

• 1、 Hudlicky, Milos. "REACTION OF ALKYL 2-CHLORO-1,1,2-TRIFLUOROETHYL ETHERS WITH LEWIS ACIDS". . p. 349 - 354. Retrieved 2007/10/02.